4RAY
Crystal structure of Magnetospirillum gryphiswaldense MSR-1 Apo-Fur
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SSRF BEAMLINE BL17U |
| Synchrotron site | SSRF |
| Beamline | BL17U |
| Temperature [K] | 130 |
| Detector technology | CCD |
| Collection date | 2011-01-26 |
| Detector | ADSC QUANTUM 315 |
| Wavelength(s) | 0.97914 |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 69.192, 78.151, 66.316 |
| Unit cell angles | 90.00, 108.47, 90.00 |
Refinement procedure
| Resolution | 50.000 - 1.550 |
| R-factor | 0.18464 |
| Rwork | 0.183 |
| R-free | 0.20815 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.008 |
| RMSD bond angle | 1.785 |
| Data reduction software | HKL-2000 |
| Data scaling software | HKL-2000 |
| Phasing software | SOLVE |
| Refinement software | REFMAC (5.6.0117) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 50.000 | 1.580 |
| High resolution limit [Å] | 1.550 | 1.550 |
| Number of reflections | 48369 | |
| Completeness [%] | 99.5 | 100 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 6 | 277 | pH 6.0, VAPOR DIFFUSION, HANGING DROP, temperature 277K |
