4R9A

Crystal structure of Human galectin-3 CRD in complex with lactose (pH 7.0, PEG4000)

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SSRF BEAMLINE BL17U
Synchrotron site	SSRF
Beamline	BL17U
Temperature [K]	100
Wavelength(s)	0.9792
Spacegroup name	P 21 21 21
Unit cell lengths	36.668, 57.920, 63.032
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	31.695 - 1.197
R-factor	0.1761
Rwork	0.175
R-free	0.19070
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.006
RMSD bond angle	1.294
Refinement software	PHENIX ((phenix.refine: 1.9_1692))

Data quality characteristics

	Overall
High resolution limit [Å]	1.197
Number of reflections	42400

Crystallization Conditions

crystal ID	method	pH	temperature	details
1