4R3M

Crystal structure of Human Hsp90 with JR9

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SSRF BEAMLINE BL17U
Synchrotron site	SSRF
Beamline	BL17U
Temperature [K]	100
Detector technology	CCD
Collection date	2013-05-18
Detector	ADSC QUANTUM 315r
Wavelength(s)	0.97947
Spacegroup name	I 2 2 2
Unit cell lengths	66.578, 90.926, 98.894
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	33.467 - 1.800
R-factor	0.211
Rwork	0.209
R-free	0.23450
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.007
RMSD bond angle	1.103
Data reduction software	HKL-2000
Data scaling software	HKL-2000
Phasing software	PHENIX
Refinement software	PHENIX ((phenix.refine: 1.8.1_1168))

Data quality characteristics

	Overall
Low resolution limit [Å]	33.467
High resolution limit [Å]	1.800
Rmerge	0.055
Number of reflections	28091
Completeness [%]	99.9
Redundancy	8.5

Crystallization Conditions

crystal ID	method	pH	temperature	details
1