Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | ALS BEAMLINE 8.3.1 |
| Synchrotron site | ALS |
| Beamline | 8.3.1 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2003-01-01 |
| Detector | ADSC QUANTUM 210 |
| Wavelength(s) | 1.1 |
| Spacegroup name | C 2 2 21 |
| Unit cell lengths | 46.283, 68.786, 137.216 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 68.600 - 1.690 |
| R-factor | 0.19637 |
| Rwork | 0.192 |
| R-free | 0.23334 |
| Structure solution method | MIR |
| RMSD bond length | 0.012 |
| RMSD bond angle | 1.524 |
| Data reduction software | DENZO |
| Data scaling software | SCALEPACK |
| Phasing software | SOLVE |
| Refinement software | REFMAC (5.8.0073) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 68.600 | 1.760 |
| High resolution limit [Å] | 1.700 | 1.700 |
| Number of reflections | 24700 | |
| <I/σ(I)> | 29.6 | 2.6 |
| Completeness [%] | 99.6 | 98.9 |
| Redundancy | 6.3 | 6.2 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 4 | 295 | 35-40% PEG 2000, 100 mM SODIUM ACETATE, 200 mM AMMONIUM ACETATE, pH 4.0, VAPOR DIFFUSION, HANGING DROP, temperature 295K |
