4QYS
TrpB2 enzymes
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SLS BEAMLINE X06DA |
| Synchrotron site | SLS |
| Beamline | X06DA |
| Detector technology | PIXEL |
| Detector | DECTRIS PILATUS 2M-F |
| Wavelength(s) | 1 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 55.564, 61.903, 109.574 |
| Unit cell angles | 90.00, 98.23, 90.00 |
Refinement procedure
| Resolution | 46.438 - 1.939 |
| R-factor | 0.1975 |
| Rwork | 0.195 |
| R-free | 0.25230 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.008 |
| RMSD bond angle | 1.088 |
| Refinement software | PHENIX ((phenix.refine: dev_1589)) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 46.438 |
| High resolution limit [Å] | 1.900 |
| Number of reflections | 52794 |
| Completeness [%] | 96.0 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | VAPOR DIFFUSION, HANGING DROP |
