4QQL

Crystal structure of C1QL3 in P1 space group

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SSRL BEAMLINE BL11-1
Synchrotron site	SSRL
Beamline	BL11-1
Temperature [K]	100
Detector technology	PIXEL
Collection date	2013-07-25
Detector	DECTRIS PILATUS 6M
Wavelength(s)	0.97945
Spacegroup name	P 1
Unit cell lengths	51.590, 82.600, 86.200
Unit cell angles	61.44, 84.50, 74.93

Refinement procedure

Resolution	46.342 - 2.390
R-factor	0.2256
Rwork	0.224
R-free	0.25870
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.004
RMSD bond angle	0.827
Refinement software	PHENIX ((phenix.refine: 1.9_1692))

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	49.790
High resolution limit [Å]	2.390	2.390
Rmerge	0.060	0.202
Number of reflections	31044
<I/σ(I)>	6.4	3.3
Completeness [%]	65.0	69.9
Redundancy		1.6

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP	6.5	292.15	0.2M Magnesium acetate tetrahydrate, 0.1M Sodium cacodylate trihydrate, 20% Polyethylene glycol 8,000, pH 6.5, VAPOR DIFFUSION, HANGING DROP, temperature 292.15K