4QQH

Crystal structure of C1QL3 in space group H32

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SSRL BEAMLINE BL12-2
Synchrotron site	SSRL
Beamline	BL12-2
Temperature [K]	100
Detector technology	PIXEL
Collection date	2010-07-20
Detector	DECTRIS PILATUS 6M
Wavelength(s)	0.9537
Spacegroup name	H 3 2
Unit cell lengths	76.230, 76.230, 125.407
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	31.921 - 1.200
R-factor	0.1544
Rwork	0.154
R-free	0.16740
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.007
RMSD bond angle	1.136
Data reduction software	XDS
Data scaling software	SCALA
Phasing software	PHASER
Refinement software	PHENIX ((phenix.refine: 1.9_1692))

Data quality characteristics

	Overall
Low resolution limit [Å]	38.110
High resolution limit [Å]	1.200
Number of reflections	41170
Completeness [%]	93.6

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP	4.6	292.15	30% PEG400, 0.1 Na-acetate, 0.01M CdCl2, pH 4.6, VAPOR DIFFUSION, HANGING DROP, temperature 292.15K