4QQ2

Crystal structure of C1QL1

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	ALS BEAMLINE 8.2.2
Synchrotron site	ALS
Beamline	8.2.2
Temperature [K]	100
Detector technology	PIXEL
Collection date	2012-08-07
Detector	DECTRIS PILATUS 6M
Wavelength(s)	0.979450
Spacegroup name	P 21 21 21
Unit cell lengths	53.072, 71.414, 85.972
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	38.169 - 1.801
R-factor	0.1665
Rwork	0.165
R-free	0.19950
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.008
RMSD bond angle	1.208
Data reduction software	XDS
Data scaling software	SCALA
Phasing software	PHASER
Refinement software	PHENIX ((phenix.refine: 1.9_1692))

Data quality characteristics

	Overall
Low resolution limit [Å]	38.169
High resolution limit [Å]	1.800
Number of reflections	30852
Completeness [%]	99.7

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP	4.3	292.15	0.2M CdCl2, 40%MPD, pH 4.3, VAPOR DIFFUSION, HANGING DROP, temperature 292.15K