4Q9C
IgNAR antibody domain C3
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | BRUKER AXS MICROSTAR |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2009-08-12 |
Detector | Bruker Platinum 135 |
Wavelength(s) | 1.514 |
Spacegroup name | P 63 2 2 |
Unit cell lengths | 99.148, 99.148, 52.281 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 15.000 - 2.800 |
R-factor | 0.25975 |
Rwork | 0.259 |
R-free | 0.28720 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4q97 |
RMSD bond length | 0.004 |
RMSD bond angle | 0.919 |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | PHASER |
Refinement software | REFMAC (5.7.0029) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 30.000 | 2.900 |
High resolution limit [Å] | 2.800 | 2.800 |
Rmerge | 0.036 | 0.304 |
Number of reflections | 4052 | |
<I/σ(I)> | 22.5 | 3.6 |
Completeness [%] | 100.0 | 100 |
Redundancy | 5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 5 | 293 | 1.0 M lithium chloride, 0.1 M citric acid, 20% PEG6000, pH 5.0, VAPOR DIFFUSION, HANGING DROP, temperature 293K |