4Q7K

Structure of NBD287 of TM287/288

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SLS BEAMLINE X06SA
Synchrotron site	SLS
Beamline	X06SA
Temperature [K]	90
Detector technology	PIXEL
Collection date	2012-02-24
Detector	PSI PILATUS 6M
Wavelength(s)	1.000
Spacegroup name	P 65 2 2
Unit cell lengths	80.170, 80.170, 129.570
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	47.367 - 1.800
R-factor	0.2046
Rwork	0.204
R-free	0.21150
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.007
RMSD bond angle	1.126
Data reduction software	XDS
Data scaling software	XSCALE
Phasing software	PHASER
Refinement software	PHENIX ((phenix.refine: 1.9_1678))

Data quality characteristics

	Overall
Low resolution limit [Å]	47.367
High resolution limit [Å]	1.800
Number of reflections	23505
Completeness [%]	100.0

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP	7.8	293.15	100 mM Tris-HCl, 100 mM sodium acetate, 25 % PEG2000 MME, pH 7.8, VAPOR DIFFUSION, HANGING DROP, temperature 293.15K