4Q4V
Crystal structure of Coxsackievirus A24v
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | DIAMOND BEAMLINE I03 |
| Synchrotron site | Diamond |
| Beamline | I03 |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2012-09-26 |
| Detector | DECTRIS PILATUS 6M |
| Spacegroup name | P 31 2 1 |
| Unit cell lengths | 303.259, 303.259, 763.592 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 99.260 - 2.900 |
| R-factor | 0.189 |
| Rwork | 0.189 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.005 |
| RMSD bond angle | 1.064 |
| Data reduction software | XDS |
| Data scaling software | XSCALE |
| Phasing software | PYMOL |
| Refinement software | REFMAC (5.8.0049) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 99.260 |
| High resolution limit [Å] | 2.900 |
| Number of reflections | 826150 |
| Completeness [%] | 92.7 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | 4.5 | 277 | 20mM Calcium chloride, 100mM Sodium acetate, 30% (w/v) MPD, pH 4.5, VAPOR DIFFUSION, HANGING DROP, temperature 277K |
