4PXB

The crystal structure of AtUAH in complex with (S)-ureidoglycolate

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	PAL/PLS BEAMLINE 7A (6B, 6C1)
Synchrotron site	PAL/PLS
Beamline	7A (6B, 6C1)
Detector technology	CCD
Detector	ADSC QUANTUM 270r
Wavelength(s)	0.97934
Spacegroup name	P 21 21 21
Unit cell lengths	70.015, 89.520, 163.061
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	30.642 - 1.903
R-factor	0.1627
Rwork	0.162
R-free	0.18850
Structure solution method	MAD
RMSD bond length	0.007
RMSD bond angle	1.089
Data reduction software	DENZO
Data scaling software	SCALEPACK
Refinement software	PHENIX (1.7.2_869)

Data quality characteristics

	Overall	Inner shell	Outer shell
Low resolution limit [Å]	50.000	50.000	1.970
High resolution limit [Å]	1.900	4.090	1.900
Rmerge	0.164	0.072	0.688
Number of reflections	80858
<I/σ(I)>	4.3
Completeness [%]	99.8	99.7	99.5
Redundancy	13.9	13.8	13.7

Crystallization Conditions

crystal ID	method	pH	temperature	details
1
1