4PTT
Crystal Structure of anti-23F strep Fab C05
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU MICROMAX-007 HF |
Temperature [K] | 93 |
Detector technology | IMAGE PLATE |
Collection date | 2013-09-09 |
Detector | RIGAKU RAXIS IV++ |
Wavelength(s) | 1.5418 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 132.140, 48.760, 80.000 |
Unit cell angles | 90.00, 120.82, 90.00 |
Refinement procedure
Resolution | 35.700 - 1.800 |
R-factor | 0.1723 |
Rwork | 0.171 |
R-free | 0.19620 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | HIE |
RMSD bond length | 0.007 |
RMSD bond angle | 1.152 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHASER |
Refinement software | PHENIX ((phenix.refine: 1.8.3_1479)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 35.700 | 1.850 |
High resolution limit [Å] | 1.800 | 1.800 |
Number of reflections | 40261 | |
<I/σ(I)> | 44.7 | 25.3 |
Completeness [%] | 98.6 | 97.5 |
Redundancy | 1.82 | 1.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 4.5 | 298 | 0.1M Na Acetate, 20% PEG 1500, pH 4.5, VAPOR DIFFUSION, HANGING DROP, temperature 298.0K |