Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | CHESS BEAMLINE F1 |
| Synchrotron site | CHESS |
| Beamline | F1 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 1998-01-01 |
| Detector | ADSC QUANTUM 4 |
| Wavelength(s) | 0.9209 |
| Spacegroup name | H 3 2 |
| Unit cell lengths | 109.350, 109.350, 190.680 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 18.577 - 2.300 |
| R-factor | 0.2028 |
| Rwork | 0.199 |
| R-free | 0.24080 |
| RMSD bond length | 0.005 |
| RMSD bond angle | 0.678 |
| Data reduction software | DENZO |
| Data scaling software | SCALEPACK |
| Phasing software | SHARP |
| Refinement software | PHENIX ((phenix.refine: 1.8.4_1496)) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 20.000 | 2.400 |
| High resolution limit [Å] | 2.300 | 2.300 |
| Rmerge | 0.066 | 0.041 |
| Number of reflections | 18903 | |
| <I/σ(I)> | 25.9 | |
| Completeness [%] | 95.6 | 96.5 |
| Redundancy | 3.84 | 3.84 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 7 | 298 | PEG MME 2000, LITHIUM SULPHATE, SPERMINE, TRIS, COBALT HEXAMMINE, MAGNESIUM CHLORIDE, pH 7.0, VAPOR DIFFUSION, SITTING DROP, temperature 298K |
