4PO4
Crystal Structure of Lampetra planeri VLRC
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | ROTATING ANODE |
| Source details | RIGAKU |
| Temperature [K] | 100 |
| Detector technology | IMAGE PLATE |
| Collection date | 2013-01-01 |
| Detector | RIGAKU RAXIS IV++ |
| Wavelength(s) | 1.5418 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 59.319, 59.542, 66.324 |
| Unit cell angles | 90.00, 108.35, 90.00 |
Refinement procedure
| Resolution | 38.570 - 2.500 |
| R-factor | 0.2127 |
| Rwork | 0.211 |
| R-free | 0.24920 |
| RMSD bond length | 0.021 |
| RMSD bond angle | 1.860 |
| Data reduction software | d*TREK (9.9.8.6 W9RSSI) |
| Data scaling software | CrystalClear |
| Phasing software | PHASER (MR) |
| Refinement software | PHENIX (1.8_1069) |
Data quality characteristics
| Overall | Inner shell | Outer shell | |
| Low resolution limit [Å] | 38.570 | 38.570 | 2.590 |
| High resolution limit [Å] | 2.500 | 5.380 | 2.500 |
| Rmerge | 0.085 | 0.056 | 0.176 |
| Total number of observations | 11640 | 11163 | |
| Number of reflections | 15329 | ||
| <I/σ(I)> | 16.1 | 27.9 | 9.4 |
| Completeness [%] | 99.7 | 99.8 | 99.2 |
| Redundancy | 7.4 | 7.28 | 7.35 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 9 | 298 | 0.1M SPG pH9, 20% PEG 1500, VAPOR DIFFUSION, HANGING DROP, temperature 298K |
