4PML
Crystal Structure of human Tankyrase 2 in complex with 3-amino-benzamide.
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | APS BEAMLINE 17-ID |
| Synchrotron site | APS |
| Beamline | 17-ID |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2009-05-12 |
| Detector | ADSC QUANTUM 210 |
| Wavelength(s) | 1.000 |
| Spacegroup name | P 21 21 21 |
| Unit cell lengths | 74.020, 79.800, 153.820 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 44.340 - 1.870 |
| R-factor | 0.2011 |
| Rwork | 0.201 |
| R-free | 0.22340 |
| RMSD bond length | 0.007 |
| RMSD bond angle | 0.890 |
| Refinement software | BUSTER (2.10.0) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 44.340 | 1.970 |
| High resolution limit [Å] | 1.870 | 1.870 |
| Number of reflections | 72922 | |
| <I/σ(I)> | 14.83 | 2 |
| Completeness [%] | 95.8 | 77.8 |
| Redundancy | 6.42 | 3.3 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 7.5 | 293 | 0.2M NaCl, 0.1M Sodium, Hepes buffer at pH7.5, 12-15% iso-propanol |
