4PLJ
Hepatitis E Virus E2s domain (Genotype IV) in complex with a neutralizing antibody 8G12
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SSRF BEAMLINE BL17U |
| Synchrotron site | SSRF |
| Beamline | BL17U |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2011-12-10 |
| Detector | ADSC QUANTUM 315r |
| Wavelength(s) | 1.0 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 56.775, 89.459, 137.636 |
| Unit cell angles | 90.00, 95.90, 90.00 |
Refinement procedure
| Resolution | 29.137 - 2.300 |
| R-factor | 0.1888 |
| Rwork | 0.187 |
| R-free | 0.24220 |
| RMSD bond length | 0.008 |
| RMSD bond angle | 1.158 |
| Refinement software | PHENIX (1.9_1692) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 30.000 |
| High resolution limit [Å] | 2.300 |
| Number of reflections | 61168 |
| <I/σ(I)> | 14.3 |
| Completeness [%] | 99.8 |
| Redundancy | 5.7 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION | 294 | 14% PEG 1500 |
