4PHR

Domain of unknown function 1792 (DUF1792) with manganese

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	APS BEAMLINE 22-ID
Synchrotron site	APS
Beamline	22-ID
Temperature [K]	100
Detector technology	CCD
Collection date	2011-03-07
Detector	MAR CCD 165 mm
Wavelength(s)	1.0000
Spacegroup name	C 1 2 1
Unit cell lengths	71.474, 45.409, 78.782
Unit cell angles	90.00, 109.74, 90.00

Refinement procedure

Resolution	37.640 - 1.340
R-factor	0.149
Rwork	0.147
R-free	0.18800
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.005
RMSD bond angle	1.153
Refinement software	PHENIX ((PHENIX.REFINE: 1.7.1_743))

Data quality characteristics

	Overall
Low resolution limit [Å]	50.000
High resolution limit [Å]	1.340
Number of reflections	52820
<I/σ(I)>	52.6
Completeness [%]	98.6
Redundancy	5.5

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP		293	Tris buffer, PEG 1500, NaAcetate