Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | APS BEAMLINE 17-BM |
| Synchrotron site | APS |
| Beamline | 17-BM |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2007-02-26 |
| Detector | MAR CCD 165 mm |
| Wavelength(s) | 1 |
| Spacegroup name | H 3 |
| Unit cell lengths | 67.205, 67.205, 127.310 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 18.870 - 1.730 |
| R-factor | 0.1871 |
| Rwork | 0.186 |
| R-free | 0.21050 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 2P92 |
| RMSD bond length | 0.010 |
| RMSD bond angle | 0.990 |
| Refinement software | BUSTER (2.10.0) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 50.000 | 1.790 |
| High resolution limit [Å] | 1.730 | 1.730 |
| Rmerge | 0.033 | 0.359 |
| Number of reflections | 22209 | |
| <I/σ(I)> | 17.8 | 3.35 |
| Completeness [%] | 99.2 | 99.5 |
| Redundancy | 3.6 | 3.3 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 7.2 | 298 | 31% PEG400, 0.2M Magnesium chloride, 0.1M HEPES, pH7.2, VAPOR DIFFUSION, SITTING DROP, temperature 298K |
