4PDN
Crystal structure of E. coli YfcM
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SPRING-8 BEAMLINE BL32XU |
| Synchrotron site | SPring-8 |
| Beamline | BL32XU |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2012-10-19 |
| Detector | RAYONIX MX225HE |
| Wavelength(s) | 1.0 |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 124.360, 36.968, 37.636 |
| Unit cell angles | 90.00, 101.22, 90.00 |
Refinement procedure
| Resolution | 36.917 - 1.448 |
| R-factor | 0.1491 |
| Rwork | 0.148 |
| R-free | 0.17450 |
| RMSD bond length | 0.005 |
| RMSD bond angle | 0.953 |
| Refinement software | PHENIX ((phenix.refine: 1.8.3_1479)) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 50.000 |
| High resolution limit [Å] | 1.448 |
| Number of reflections | 29327 |
| <I/σ(I)> | 45.4 |
| Completeness [%] | 97.5 |
| Redundancy | 5.8 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 293 | PEG 3350, ammonium sulfate, Bis-Tris |
