4PAL

IONIC INTERACTIONS WITH PARVALBUMINS. CRYSTAL STRUCTURE DETERMINATION OF PIKE 4.10 PARVALBUMIN IN FOUR DIFFERENT IONIC ENVIRONMENTS

Experimental procedure

Spacegroup name	P 41 21 2
Unit cell lengths	57.500, 57.500, 87.400
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	7.000 * - 1.800
Rwork	0.180
RMSD bond length	0.030
RMSD bond angle	2.900
Refinement software	EREF

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	9999.000 *
High resolution limit [Å]	1.800 *	1.800 *
Rmerge	0.089 *
Total number of observations	64669 *
Number of reflections	13286 *
Completeness [%]	89.0 *	85 *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	reservoir	sodium azide	3 (mM)