4P9N
Crystal structure of sshesti PE mutant
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | ROTATING ANODE |
| Source details | RIGAKU MICROMAX-007 HF |
| Temperature [K] | 90 |
| Detector technology | IMAGE PLATE |
| Collection date | 2008-06-26 |
| Detector | RIGAKU RAXIS VII |
| Wavelength(s) | 1.5418 |
| Spacegroup name | I 2 2 2 |
| Unit cell lengths | 59.036, 71.748, 137.862 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 38.024 - 1.800 |
| R-factor | 0.15403 |
| Rwork | 0.152 |
| R-free | 0.18655 |
| RMSD bond length | 0.018 |
| RMSD bond angle | 1.780 |
| Refinement software | REFMAC (5.8.0069) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 50.000 |
| High resolution limit [Å] | 1.800 |
| Number of reflections | 27484 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION | 293 | 12% PEG 3000, 100MM PHOSPHATE-CITRATE, 200MM NACL |
