4P98
ABC transporter system solute-bindng protein from Conexibacter woesei DSM 14684
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 19-ID |
Synchrotron site | APS |
Beamline | 19-ID |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2013-08-19 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.91975 |
Spacegroup name | P 41 21 2 |
Unit cell lengths | 79.091, 79.091, 139.713 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 24.680 - 1.900 |
R-factor | 0.1592 |
Rwork | 0.157 |
R-free | 0.20310 |
RMSD bond length | 0.007 |
RMSD bond angle | 1.162 |
Data scaling software | SCALEPACK |
Refinement software | REFMAC (5.7.0029) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 50.000 | 50.000 | 1.930 |
High resolution limit [Å] | 1.900 | 5.160 | 1.900 |
Rmerge | 0.071 | 0.036 | 0.820 |
Total number of observations | 495004 | ||
Number of reflections | 35740 | ||
<I/σ(I)> | 11.8 | ||
Completeness [%] | 99.9 | 97.6 | 100 |
Redundancy | 13.9 | 12 | 12.1 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 8.5 | 289 | 2.0 M Ammonium Sulfate, 0.1 M Tris-Cl |