4P4K

Structural Basis of Chronic Beryllium Disease: Bridging the Gap Between allergic hypersensitivity and auto immunity

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	NSLS BEAMLINE X26C
Synchrotron site	NSLS
Beamline	X26C
Temperature [K]	100
Detector technology	PIXEL
Collection date	2012-08-13
Detector	PSI PILATUS 6M
Wavelength(s)	1.1
Spacegroup name	P 21 21 21
Unit cell lengths	79.400, 137.240, 213.130
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	39.700 - 2.800
R-factor	0.2064
Rwork	0.204
R-free	0.25180
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	3lqz
RMSD bond length	0.010
RMSD bond angle	1.390
Refinement software	BUSTER (2.10.0)

Data quality characteristics

	Overall
Low resolution limit [Å]	40.000
High resolution limit [Å]	2.800
Number of reflections	58169
<I/σ(I)>	15.67
Completeness [%]	99.9
Redundancy	14

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, SITTING DROP		293	PEG8K, Na Cacodylate, glycerol