4P2N
Structure of the P domain from a GI.7 Norovirus variant in complex with LeX HBGA
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | ALS BEAMLINE 5.0.1 |
| Synchrotron site | ALS |
| Beamline | 5.0.1 |
| Temperature [K] | 77 |
| Detector technology | CCD |
| Collection date | 2012-12-17 |
| Detector | ADSC QUANTUM 315r |
| Wavelength(s) | 0.97935 |
| Spacegroup name | P 1 |
| Unit cell lengths | 62.267, 63.031, 90.278 |
| Unit cell angles | 99.02, 98.16, 119.51 |
Refinement procedure
| Resolution | 45.954 - 1.700 |
| R-factor | 0.1561 |
| Rwork | 0.155 |
| R-free | 0.17140 |
| RMSD bond length | 0.008 |
| RMSD bond angle | 1.238 |
| Refinement software | PHENIX ((phenix.refine: 1.8.1_1168)) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 50.000 |
| High resolution limit [Å] | 1.700 |
| Number of reflections | 122585 |
| <I/σ(I)> | 16.84 |
| Completeness [%] | 97.5 |
| Redundancy | 3.9 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 6.5 | 293 | 0.2M Sodium Formate 0.1M Bis Tris Propane 20% PEG3350 |
