4OZ5
Bacillus subtilis HmoB
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | PAL/PLS BEAMLINE 5C (4A) |
| Synchrotron site | PAL/PLS |
| Beamline | 5C (4A) |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2012-05-08 |
| Detector | ADSC QUANTUM 270 |
| Wavelength(s) | 1.000 |
| Spacegroup name | I 2 3 |
| Unit cell lengths | 99.597, 99.597, 99.597 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 19.530 - 2.710 |
| R-factor | 0.19673 |
| Rwork | 0.193 |
| R-free | 0.27138 |
| RMSD bond length | 0.012 |
| RMSD bond angle | 1.603 |
| Refinement software | REFMAC (5.7.0029) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 30.000 |
| High resolution limit [Å] | 2.700 |
| Number of reflections | 4635 |
| <I/σ(I)> | 45.6 |
| Completeness [%] | 100.0 |
| Redundancy | 25 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 293 | 1.3 M Sodium Citrate, 0.5% PEG 2000, 0.1 M HEPES pH 7.0 |
