4OY8

Structure of ScLPMO10B in complex with zinc.

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	ESRF BEAMLINE ID14-4
Synchrotron site	ESRF
Beamline	ID14-4
Temperature [K]	100
Detector technology	CCD
Collection date	2013-03-01
Detector	ADSC QUANTUM 315
Wavelength(s)	1.28
Spacegroup name	P 31 2 1
Unit cell lengths	67.620, 67.620, 107.290
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	35.790 - 1.400
R-factor	0.12588
Rwork	0.125
R-free	0.14333
RMSD bond length	0.011
RMSD bond angle	1.400
Refinement software	REFMAC (5.7.0032)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	35.000	1.480
High resolution limit [Å]	1.400	1.400
Rmerge	0.080	0.228
Number of reflections	54273
<I/σ(I)>	13.6	3.6
Completeness [%]	96.0	76.7
Redundancy	4.5	2

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP	6.5	293	0.2 M zinc acetate, 0.1 M sodium cacodylate, 9 % v/v 2-propanol