4OW2
YopM from Yersinia enterocolitica WA-314
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | PETRA III, EMBL c/o DESY BEAMLINE P14 (MX2) |
| Synchrotron site | PETRA III, EMBL c/o DESY |
| Beamline | P14 (MX2) |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2013-09-29 |
| Detector | PSI PILATUS 6M |
| Wavelength(s) | 0.979570 |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 210.847, 126.290, 139.933 |
| Unit cell angles | 90.00, 118.26, 90.00 |
Refinement procedure
| Resolution | 30.000 - 3.200 |
| R-factor | 0.18251 |
| Rwork | 0.181 |
| R-free | 0.20124 |
| RMSD bond length | 0.006 |
| RMSD bond angle | 1.234 |
| Refinement software | REFMAC (5.8.0049) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 50.000 |
| High resolution limit [Å] | 3.200 |
| Number of reflections | 64045 |
| <I/σ(I)> | 14.2 |
| Completeness [%] | 97.0 |
| Redundancy | 6.59 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 293 | BisTris Propane, sodium citrate, PEG 3350 |
