4OTS
Crystal Structure of isolated Operophtera brumata CPV18
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | DIAMOND BEAMLINE I24 |
| Synchrotron site | Diamond |
| Beamline | I24 |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2011-07-28 |
| Detector | DECTRIS PILATUS 6M |
| Wavelength(s) | 0.9686 |
| Spacegroup name | I 2 3 |
| Unit cell lengths | 102.794, 102.794, 102.794 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 27.473 - 1.704 |
| R-factor | 0.1018 |
| Rwork | 0.100 |
| R-free | 0.13150 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.006 |
| RMSD bond angle | 1.169 |
| Data reduction software | FastDP |
| Data scaling software | Blend |
| Phasing software | PHASER |
| Refinement software | PHENIX ((phenix.refine: 1.8.4_1496)) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 72.686 | |
| High resolution limit [Å] | 1.700 | 1.700 |
| Number of reflections | 19343 | |
| Completeness [%] | 97.2 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | 7.5 | 301 | Crystals formed naturally within the cytoplasm and were purified from cells, pH 7.5, temperature 301K |
