4OPF
Streptomcyes albus JA3453 oxazolomycin ketosynthase domain OzmH KS8
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 19-ID |
Synchrotron site | APS |
Beamline | 19-ID |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2013-08-20 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.9792 |
Spacegroup name | P 43 3 2 |
Unit cell lengths | 145.922, 145.922, 145.922 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 46.145 - 2.120 |
R-factor | 0.15701 |
Rwork | 0.156 |
R-free | 0.17905 |
Structure solution method | SAD |
RMSD bond length | 0.016 |
RMSD bond angle | 1.693 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | SHELXD |
Refinement software | REFMAC (5.7.0029) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 46.200 | 50.000 | 2.160 |
High resolution limit [Å] | 2.120 | 5.750 | 2.120 |
Rmerge | 0.117 | 0.048 | 0.957 |
Number of reflections | 30731 | ||
<I/σ(I)> | 7.8 | 3.9 | |
Completeness [%] | 100.0 | 99.9 | 100 |
Redundancy | 20.3 | 17.9 | 17.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 7.5 | 297 | o.2 M ammonium sulfate, 0.1 M Hepes buffer, 25% PEG-3350, pH 7.5, VAPOR DIFFUSION, SITTING DROP, temperature 297K |