4OKX

Crystal structure of W741L-AR-LBD bound with co-regulator peptide

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	NSRRC BEAMLINE BL13B1
Synchrotron site	NSRRC
Beamline	BL13B1
Temperature [K]	150
Detector technology	CCD
Detector	ADSC QUANTUM 315
Wavelength(s)	1.0
Spacegroup name	P 21 21 21
Unit cell lengths	55.861, 66.674, 70.291
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	27.180 - 2.100
R-factor	0.19949
Rwork	0.197
R-free	0.24769
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	4ojb
RMSD bond length	0.017
RMSD bond angle	1.850
Data reduction software	HKL-2000
Data scaling software	SCALEPACK
Phasing software	AMoRE
Refinement software	REFMAC (5.6.0117)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	48.370	2.180
High resolution limit [Å]	2.100	2.100
Rmerge	0.036	0.209
Number of reflections	15864
<I/σ(I)>	41.7	10.4
Completeness [%]	99.8	100
Redundancy	6

Crystallization Conditions

crystal ID	method	pH	temperature	details
1