4OFK
Crystal Structure of SYG-2 D4
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SSRL BEAMLINE BL11-1 |
| Synchrotron site | SSRL |
| Beamline | BL11-1 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2011-07-05 |
| Detector | MARMOSAIC 325 mm CCD |
| Wavelength(s) | 1.16962 |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 61.812, 54.131, 63.623 |
| Unit cell angles | 90.00, 104.61, 90.00 |
Refinement procedure
| Resolution | 40.135 - 1.802 |
| R-factor | 0.1923 |
| Rwork | 0.191 |
| R-free | 0.21060 |
| Structure solution method | SAD |
| RMSD bond length | 0.005 |
| RMSD bond angle | 1.044 |
| Data reduction software | HKL-2000 |
| Data scaling software | HKL-2000 |
| Phasing software | PHASER |
| Refinement software | PHENIX ((phenix.refine: 1.8.4_1496)) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 50.000 |
| High resolution limit [Å] | 1.800 |
| Number of reflections | 18855 |
| <I/σ(I)> | 24.3 |
| Completeness [%] | 100.0 |
| Redundancy | 3.8 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 8.3 | 295 | 1.3 M Ammonium sulfate, 0.1 M Tris pH 8.3, VAPOR DIFFUSION, SITTING DROP, temperature 295.0K |
