4OFI
Crystal Structure of Duf (Kirre) D1
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRL BEAMLINE BL9-2 |
Synchrotron site | SSRL |
Beamline | BL9-2 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2010-12-02 |
Detector | MARMOSAIC 325 mm CCD |
Wavelength(s) | 1.0000 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 74.330, 84.358, 82.633 |
Unit cell angles | 90.00, 115.27, 90.00 |
Refinement procedure
Resolution | 37.503 - 2.300 |
R-factor | 0.1944 |
Rwork | 0.192 |
R-free | 0.24330 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4of8 |
RMSD bond length | 0.008 |
RMSD bond angle | 0.716 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHASER |
Refinement software | PHENIX ((phenix.refine: 1.7.1_740)) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 50.000 |
High resolution limit [Å] | 2.300 |
Number of reflections | 41218 |
<I/σ(I)> | 12.7 |
Completeness [%] | 100.0 |
Redundancy | 3.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 5.5 | 295 | 25% PEG 3,350, 0.2 M Sodium chloride, 0.1 M Bis-tris pH 5.5, VAPOR DIFFUSION, SITTING DROP, temperature 295.0K |