4OEA

Crystal structure of AR-LBD

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	NSRRC BEAMLINE BL13B1
Synchrotron site	NSRRC
Beamline	BL13B1
Temperature [K]	123
Detector technology	CCD
Detector	ADSC QUANTUM 315
Wavelength(s)	1.0
Spacegroup name	P 21 21 21
Unit cell lengths	55.668, 65.975, 70.796
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	24.140 - 2.120
R-factor	0.20825
Rwork	0.205
R-free	0.26549
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	1t73
RMSD bond length	0.012
RMSD bond angle	1.286
Data reduction software	HKL-2000
Data scaling software	HKL-2000
Phasing software	AMoRE
Refinement software	REFMAC (5.7.0029)

Data quality characteristics

	Overall
Low resolution limit [Å]	50.000
High resolution limit [Å]	2.100
Number of reflections	15322
Completeness [%]	96.0

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP	6.5	298	1.6M magnesium sulphate, 0.1M MES , pH 6.5, VAPOR DIFFUSION, HANGING DROP, temperature 298K