4OBT

Crystal structure of Arabidopsis thaliana cytosolic triose phosphate isomerase

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	APS BEAMLINE 17-ID
Synchrotron site	APS
Beamline	17-ID
Temperature [K]	100
Detector technology	CCD
Collection date	2013-10-12
Detector	ADSC QUANTUM 210
Wavelength(s)	1.09
Spacegroup name	P 21 21 21
Unit cell lengths	77.940, 84.590, 89.720
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	38.970 - 1.600
R-factor	0.1668
Rwork	0.166
R-free	0.18890
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.009
RMSD bond angle	1.141
Refinement software	PHENIX ((phenix.refine: 1.8.4_1496))

Data quality characteristics

	Overall
Low resolution limit [Å]	38.970
High resolution limit [Å]	1.600
Number of reflections	78784
Completeness [%]	99.9

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP	7.4	294	pH 7.4, VAPOR DIFFUSION, HANGING DROP, temperature 294K