4OAZ
BldD CTD-c-di-GMP complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ALS BEAMLINE 8.3.1 |
Synchrotron site | ALS |
Beamline | 8.3.1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2013-03-12 |
Detector | ADSC QUANTUM 315r |
Spacegroup name | C 2 2 21 |
Unit cell lengths | 36.870, 95.530, 100.120 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 34.560 - 2.250 |
R-factor | 0.243 |
Rwork | 0.236 |
R-free | 0.28400 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.006 |
RMSD bond angle | 1.359 |
Refinement software | PHENIX ((phenix.refine: 1.6.4_486)) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 34.600 |
High resolution limit [Å] | 2.250 |
Number of reflections | 8186 |
Completeness [%] | 94.0 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 6.5 | 298 | sodium/potassium phosphate, pH 6.5, VAPOR DIFFUSION, HANGING DROP, temperature 298K |