4O7J
Crystal structure of CarG
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | DIAMOND BEAMLINE I02 |
| Synchrotron site | Diamond |
| Beamline | I02 |
| Collection date | 2013-05-26 |
| Wavelength(s) | 0.97780 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 45.470, 66.810, 50.450 |
| Unit cell angles | 90.00, 95.69, 90.00 |
Refinement procedure
| Resolution | 30.000 - 1.800 |
| R-factor | 0.18489 |
| Rwork | 0.182 |
| R-free | 0.23693 |
| Structure solution method | SAD |
| RMSD bond length | 0.019 |
| RMSD bond angle | 1.884 |
| Data reduction software | MOSFLM |
| Data scaling software | Aimless |
| Phasing software | PHENIX |
| Refinement software | REFMAC (5.7.0032) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 33.400 | 1.770 |
| High resolution limit [Å] | 1.740 | 1.740 |
| Number of reflections | 30381 | |
| Completeness [%] | 98.0 | 87.3 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 8 | 291 | 30% PEG 1500, pH 8.0, VAPOR DIFFUSION, SITTING DROP, temperature 291K |
