4O6J

Crystal sturucture of T. acidophilum IdeR

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	PAL/PLS BEAMLINE 7A (6B, 6C1)
Synchrotron site	PAL/PLS
Beamline	7A (6B, 6C1)
Temperature [K]	100
Detector technology	CCD
Collection date	2013-10-22
Detector	ADSC QUANTUM 210
Wavelength(s)	1.7394
Spacegroup name	P 21 21 2
Unit cell lengths	61.215, 84.604, 46.956
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	19.991 - 2.300
R-factor	0.1631
Rwork	0.161
R-free	0.21030
Structure solution method	SAD
RMSD bond length	0.010
RMSD bond angle	1.260
Data reduction software	HKL-2000
Data scaling software	HKL-2000
Phasing software	SOLVE
Refinement software	PHENIX ((phenix.refine: 1.8.4_1496))

Data quality characteristics

	Overall
Low resolution limit [Å]	19.991
High resolution limit [Å]	2.300
Number of reflections	11321
Completeness [%]	99.1

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP	4.5	296	20% PEG 4000, 0.2M ammonium acetate, 0.1M sodium acetate , pH 4.5, VAPOR DIFFUSION, HANGING DROP, temperature 296K