4O5V

Crystal structure of T. acidophilum IdeR

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	PAL/PLS BEAMLINE 5C (4A)
Synchrotron site	PAL/PLS
Beamline	5C (4A)
Temperature [K]	100
Detector technology	CCD
Collection date	2012-05-15
Detector	ADSC QUANTUM 315r
Wavelength(s)	0.9792
Spacegroup name	P 21 21 2
Unit cell lengths	61.198, 84.978, 47.078
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	34.166 - 2.100
R-factor	0.182
Rwork	0.182
R-free	0.22500
Structure solution method	SAD
RMSD bond length	0.009
RMSD bond angle	1.190
Data reduction software	HKL-2000
Data scaling software	HKL-2000
Phasing software	SOLVE
Refinement software	PHENIX ((phenix.refine: 1.8.4_1496))

Data quality characteristics

	Overall
Low resolution limit [Å]	50.000
High resolution limit [Å]	2.100
Number of reflections	14925
Completeness [%]	99.9

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP	4.5	296	20% PEG 4000, pH 4.5, VAPOR DIFFUSION, HANGING DROP, temperature 296K