4NHS
X-ray structure of the complex between hen egg white lysozyme and pentachlorocarbonyliridate(III) (9 days)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU MICROMAX-007 HF |
Temperature [K] | 100 |
Collection date | 2012-10-14 |
Wavelength(s) | 1.5418 |
Spacegroup name | P 43 21 2 |
Unit cell lengths | 77.681, 77.681, 37.041 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 22.060 - 1.990 |
R-factor | 0.2567 |
Rwork | 0.229 |
R-free | 0.29870 |
Structure solution method | FOURIER SYNTHESIS |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | CNS |
Refinement software | CNS |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 54.929 |
High resolution limit [Å] | 1.940 |
Number of reflections | 8832 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 4.5 | 298 | Ir(Cl)5CO for 9 days, pH 4.5, VAPOR DIFFUSION, HANGING DROP, temperature 298K |