4NHQ
X-ray structure of the complex between hen egg white lysozyme and pentachlorocarbonyliridate(III) (5 days)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU MICROMAX-007 HF |
Temperature [K] | 100 |
Collection date | 2012-10-10 |
Wavelength(s) | 1.5418 |
Spacegroup name | P 43 21 2 |
Unit cell lengths | 80.190, 80.190, 36.677 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 25.360 - 1.920 |
R-factor | 0.2201 |
Rwork | 0.198 |
R-free | 0.26030 |
Structure solution method | FOURIER SYNTHESIS |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | CNS |
Refinement software | CNS |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 56.703 |
High resolution limit [Å] | 1.890 |
Number of reflections | 10073 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 4.5 | 298 | Ir(Cl)5CO for 5 days, pH 4.5, VAPOR DIFFUSION, HANGING DROP, temperature 298K |