4NHP

X-ray structure of the complex between the hen egg white lysozyme and pentachlorocarbonyliridate (III) (4 days)

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	ROTATING ANODE
Source details	RIGAKU MICROMAX-007 HF
Temperature [K]	100
Wavelength(s)	1.5418
Spacegroup name	P 43 21 2
Unit cell lengths	78.441, 78.441, 37.113
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	25.490 - 1.420
R-factor	0.206
Rwork	0.188
R-free	0.22710
Structure solution method	FOURIER SYNTHESIS
Starting model (for MR)	193l
Data reduction software	HKL-2000
Data scaling software	HKL-2000
Phasing software	CNS
Refinement software	CNS

Data quality characteristics

	Overall
Low resolution limit [Å]	50.000
High resolution limit [Å]	1.420
Number of reflections	22421

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP	4.5	298	Ir(Cl)5CO, pH 4.5, VAPOR DIFFUSION, HANGING DROP, temperature 298K