4NDO
Crystal structure Molybdenum Storage Protein with fully Mo-loaded cavity
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X10SA |
Synchrotron site | SLS |
Beamline | X10SA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2012-08-18 |
Detector | PSI PILATUS 6M |
Wavelength(s) | 1.00 |
Spacegroup name | P 63 2 2 |
Unit cell lengths | 115.600, 115.600, 234.100 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 9.986 - 1.350 |
R-factor | 0.1611 |
Rwork | 0.160 |
R-free | 0.17730 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4f6t |
RMSD bond length | 0.019 |
RMSD bond angle | 1.900 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | REFMAC |
Refinement software | PHENIX ((phenix.refine: 1.8.1_1168)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 1.430 |
High resolution limit [Å] | 1.350 | 1.350 |
Number of reflections | 212763 | |
Completeness [%] | 95.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 5.6 | 291 | 0,1 M NaCitrate, 1.1 M (NH4)HCitrate, 0.1 M (NH4)H2PO4, 15% (v/v)EG, pH 5.6, VAPOR DIFFUSION, SITTING DROP, temperature 291K |