4NAC
Crystal Structure of the N-terminal Domain of p15RS
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SSRF BEAMLINE BL17U |
| Synchrotron site | SSRF |
| Beamline | BL17U |
| Detector technology | CCD |
| Detector | ADSC QUANTUM 315r |
| Wavelength(s) | 0.98000 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 43.691, 47.326, 68.019 |
| Unit cell angles | 90.00, 100.24, 90.00 |
Refinement procedure
| Resolution | 30.330 - 2.002 |
| R-factor | 0.1761 |
| Rwork | 0.174 |
| R-free | 0.21420 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.007 |
| RMSD bond angle | 0.908 |
| Data reduction software | DENZO |
| Data scaling software | SCALEPACK |
| Phasing software | PHASER |
| Refinement software | PHENIX (dev_596) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 30.330 | |
| High resolution limit [Å] | 2.002 | 2.002 |
| Number of reflections | 18187 | |
| Completeness [%] | 97.7 | 97.69 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION | 7 | 291 | 2.2M DL-Malic acid, 0.1M Bis-Tris propane, pH 7.0, VAPOR DIFFUSION, temperature 291K |
