4N8O
Crystal structure of Mycobacterial FtsX extracellular domain, bromide derivative
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | ALS BEAMLINE 8.3.1 |
| Synchrotron site | ALS |
| Beamline | 8.3.1 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2013-01-15 |
| Detector | ADSC QUANTUM 315r |
| Wavelength(s) | 0.92004 |
| Spacegroup name | I 4 |
| Unit cell lengths | 133.167, 133.167, 28.769 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 47.080 - 2.300 |
| R-factor | 0.193 |
| Rwork | 0.191 |
| R-free | 0.23900 |
| Structure solution method | SAD |
| RMSD bond length | 0.008 |
| RMSD bond angle | 0.888 |
| Data reduction software | DENZO |
| Data scaling software | SCALEPACK |
| Phasing software | CRANK2 |
| Refinement software | PHENIX (1.8.3_1479) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 50.000 |
| High resolution limit [Å] | 2.300 |
| Number of reflections | 21912 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | 8 | 291 | 25% PEG MME 2000, 150mM KBr, pH 8, VAPOR DIFFUSION, HANGING DROP, temperature 291K |
