4MZP
MazF from S. aureus crystal form III, C2221, 2.7 A
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SOLEIL BEAMLINE PROXIMA 1 |
Synchrotron site | SOLEIL |
Beamline | PROXIMA 1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2011-02-10 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 1.0394 |
Spacegroup name | C 2 2 21 |
Unit cell lengths | 90.881, 92.636, 222.376 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 39.200 - 2.702 |
R-factor | 0.2103 |
Rwork | 0.208 |
R-free | 0.24260 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4mzm |
RMSD bond length | 0.014 |
RMSD bond angle | 1.328 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | CCP4 ((Phaser)) |
Refinement software | PHENIX ((phenix.refine: 1.7_650)) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 39.200 |
High resolution limit [Å] | 2.700 |
Rmerge | 0.093 |
Number of reflections | 25526 |
<I/σ(I)> | 13.3 |
Completeness [%] | 98.0 |
Redundancy | 3.4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7.5 | 293 | 2.0 M (NH4)2SO4, 0.1 M NAAC pH 4.6, VAPOR DIFFUSION, HANGING DROP, temperature 293K |