4MMX
Integrin AlphaVBeta3 ectodomain bound to the tenth domain of Fibronectin
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 19-ID |
Synchrotron site | APS |
Beamline | 19-ID |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2012-10-13 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.97921 |
Spacegroup name | P 32 2 1 |
Unit cell lengths | 129.859, 129.859, 305.831 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 42.506 - 3.320 |
R-factor | 0.2105 |
Rwork | 0.208 |
R-free | 0.25860 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.010 |
RMSD bond angle | 0.864 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | PHASER |
Refinement software | PHENIX ((phenix.refine: 1.8.2_1309)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 75.490 | 3.410 |
High resolution limit [Å] | 3.320 | 3.320 |
Rmerge | 0.109 | |
Number of reflections | 39593 | |
<I/σ(I)> | 13.9 | 3.3 |
Completeness [%] | 88.0 | 88 |
Redundancy | 6.2 | 6.4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 4.5 | 277.15 | 12% PEG3350, 0.8 M sodium chloride, 0.1 M sodium acetate, pH 4.5, VAPOR DIFFUSION, HANGING DROP, temperature 277.15K |