4M5C
Crystal Structure of an Truncated Transition metal Transporter
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL17U |
Synchrotron site | SSRF |
Beamline | BL17U |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2013-06-03 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 1.589 |
Spacegroup name | C 2 2 21 |
Unit cell lengths | 64.479, 103.820, 121.285 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 47.723 - 2.500 |
R-factor | 0.2034 |
Rwork | 0.201 |
R-free | 0.24100 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.007 |
RMSD bond angle | 1.063 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHASES |
Refinement software | PHENIX ((phenix.refine: 1.8_1069)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | |
High resolution limit [Å] | 2.500 | 2.500 |
Number of reflections | 27181 | |
Completeness [%] | 99.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 9.8 | 291.15 | 30% PEG 400, 0.05M CAPSO, 0.05M magnesium acetate,, pH 9.8, VAPOR DIFFUSION, HANGING DROP, temperature 291.15K |