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4M2P

Crystal structure of a non-myristoylated C39D recoverin mutant with one calcium ion bound to EF-hand 3

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsALS BEAMLINE 8.2.1
Synchrotron siteALS
Beamline8.2.1
Temperature [K]100
Detector technologyCCD
Collection date2013-05-15
DetectorADSC QUANTUM 315r
Spacegroup nameI 4
Unit cell lengths84.220, 84.220, 59.600
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution29.800 - 1.450
R-factor0.205
Rwork0.204
R-free0.22200
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)1omr
RMSD bond length0.006
RMSD bond angle1.108
Data reduction softwareMOSFLM
Data scaling softwareSCALA
Phasing softwarePHASER
Refinement softwarePHENIX (1.8.2_1309)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]32.0001.530
High resolution limit [Å]1.4501.450
Rmerge0.0950.421
Number of reflections36942
<I/σ(I)>9.62.6
Completeness [%]100.0100
Redundancy4.13.6
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, HANGING DROP72962.4 M SODIUM MALONATE, pH 7.0, VAPOR DIFFUSION, HANGING DROP, temperature 296K

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