4LR2
Crystal Structure of Human ENPP4 (apo)
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | CHESS BEAMLINE A1 |
| Synchrotron site | CHESS |
| Beamline | A1 |
| Detector technology | CCD |
| Collection date | 2013-06-03 |
| Detector | ADSC QUANTUM 210 |
| Wavelength(s) | 0.978 |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 181.506, 51.293, 53.065 |
| Unit cell angles | 90.00, 102.08, 90.00 |
Refinement procedure
| Resolution | 22.730 - 1.500 |
| R-factor | 0.1566 |
| Rwork | 0.154 |
| R-free | 0.20130 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | PDB ID 2GSU WITHOUT LIGAND |
| RMSD bond length | 0.009 |
| RMSD bond angle | 1.198 |
| Data reduction software | DENZO |
| Data scaling software | SCALEPACK |
| Refinement software | PHENIX (1.8.2_1309) |
Data quality characteristics
| Overall | Inner shell | Outer shell | |
| Low resolution limit [Å] | 50.000 | 50.000 | 1.530 |
| High resolution limit [Å] | 1.500 | 3.780 | 1.500 |
| Rmerge | 0.084 | 0.056 | 0.548 |
| Number of reflections | 71681 | ||
| <I/σ(I)> | 14.3 | ||
| Completeness [%] | 93.6 | 96.2 | 60.2 |
| Redundancy | 6.8 | 7.2 | 5 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
